Tri-p-tolylphosphine

Name: Tri-p-tolylphosphine
Brand: ChemScene
Availability: InStock
Rating: 5 (1 reviews)

CAS No. 1038-95-5
Cat. No. CS-W012099
Purity≥96%
MDL No.MFCD00008542

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Type	HazMat Fee
Excepted Quantity	$0.00
FedEx Limited Quantities Ground	$0.00
Hazmat Ground shipping	$50.00+
Inaccessible (Haz class 6.1 or 9), Domestic	$68.00+
Accessible (Haz class 3, 4, 5 or 8), Domestic	$158.00+
Inaccessible (Haz class 6.1 or 9), International	$108.00+
Accessible (Haz class 3, 4, 5 or 8), International	$238.00+

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Structure of 1038-95-5

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General Information

CAS No. 1038-95-5
Cat. No. CS-W012099
Purity ≥96%
MDL No. MFCD00008542
Storage 4°C, stored under nitrogen
Shipping Room temperature in continental US; may vary elsewhere.
Molecular Formula C₂₁H₂₁P
Molecular Weight 304.37
Synonym(s) None
SMILES CC1=CC=C(C=C1)P(C2=CC=C(C=C2)C)C3=CC=C(C=C3)C

Description

N-Cyclohexylhydroxylamine hydrochloride is used in the preparation of 4-carbethoxy-2-cyclohexyl-5-(2H)-isoxazolone and hexahydroisoxazolequinoline analogs. It is also used in the preparation of N-cyclohexyl nitrone by reaction with aldehyde. Further, it acts as a hydroxylamination reagent for allyl esters. In addition to this, it serves as a reagent in the conversion of 1,2-dicarboxylic acids to alfa-beta-unsaturated carboxylic acids.

Synthesis

Route1
- In-stock
  
  797-70-6
- ~91%
- In-stock
  
  1038-95-5
References
- Li, Yuehui; Das, Shoubhik; Zhou, Shaolin; Junge, Kathrin; Beller, Matthias Journal of the American Chemical Society, 2012 , vol. 134, # 23 p. 9727 - 9732
Route2
- 21859-00-7
- ~%
- In-stock
  
  1038-95-5
References
- Tetrahedron, , vol. 67, # 32 p. 5825 - 5831
Route3
- 126403-71-2
- ~37%
- In-stock
  
  1038-95-5
References
- Le Gall, Erwan; Ben Aissi, Karima; Lachaise, Isabelle; Troupel, Michel Synlett, 2006 , # 6 p. 954 - 956

Safety Information

Download SDS

GHS Pictogram :	GHS No : GHS07
Signal Word : Warning	UN#: N/A
Class : N/A	Packing Group : N/A
Hazard Statements : H315-H319-H335
Precautionary Statements : P261-P264-P271-P280-P302+P352-P304+P340-P362+P364-P405-P501

Quality Control

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Computational Chemistry Data

TPSA 0
LogP 4.37006
H_Acceptors 0
H_Donors 0
Rotatable_Bonds 3

Other Classifications

Bioactive Molecules Dye and Bio-assay Reagents

Catalysts and Ligands Ligands Achiral Mono/Dual Phosphorus Ligands Aryl Phosphorus(Single Phosphorus) Ligands

Catalysis Cross-Coupling Buchwald Ligands and Complexes

Catalysis Cross-Coupling Phosphine Ligands

Catalysis Cross-coupling Reaction using Transition Metal Catalysts Phosphine Ligands

Catalysis Phosphorous Compounds Buchwald Ligands

Chemical Synthesis Synthetic Reagents C-C Bond Formation Cross-coupling Reaction using Transition Metal Catalysts

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Tri-p-tolylphosphine

CAS No. 1038-95-5

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