Lot numbers can be found on the outside label of a product:
Triazabicyclodecene
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CAS No. 5807-14-7
- Cat. No. CS-B0736
- Purity≥97%
- MDL No.MFCD00043003
*For research and further manufacturing use only, not for direct human use.
Structure of 5807-14-7
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General Information
- CAS No. 5807-14-7
- Cat. No. CS-B0736
- Purity ≥97%
- MDL No. MFCD00043003
- Storage 4°C, protect from light
- Shipping Room temperature in continental US; may vary elsewhere.
- Molecular Formula C₇H₁₃N₃
- Molecular Weight 139.20
- Synonym(s) None
- SMILES C12=NCCCN1CCCN2
Description
1,5,7-Triazabicyclo[4.4.0]dec-5-ene, a bicyclic guanidine base, has been found to be an excellent catalyst for Michael and Michael-type reactions. It forms 1:1 complex with lasalocid acid and crystal structure of the complex has been studied by X-ray diffraction, FT-IR spectroscopy and 1H NMR.1,5,7-Triazabicyclo[4.4.0]dec-5-ene may be used as organocatalyst for aminolysis of esters. It may be used as catalyst for direct addition of P(O)-H bonds (dialkyl phosphites and diphenyl phosphonite) across various activated alkenes. Polymer supported 1,5,7-triazabicyclo[4.4.0]dec-5-ene (PTBD) was used as a base and a reagent scavenger for the synthesis of aryl ethers from phenols and alkyl or aryl halides.
Synthesis
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Route1
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56-18-8 -
In-stock
726-42-1 - ~76%
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In-stock
5807-14-7
References
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Shen, Hao; Wang, Yang; Xie, Zuowei Organic Letters, 2011 , vol. 13, # 17 p. 4562 - 4565
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Route2
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56-18-8
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127099-85-8
- ~57%
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In-stock
5807-14-7
References
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PPG INDUSTRIES OHIO, INC.; ZAWACKY, Steven R.; HICKENBOTH, Charles R.; KARABIN, Richard F.; McCOLLUM, Gregory J.; MORIARITY, Thomas C. Patent: WO2011/112594 A1, 2011 ; Location in patent: Page/Page column 18-19 ;
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Route3
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56-18-8
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In-stock
50-01-1 - ~90%
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In-stock
5807-14-7
References
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Usachev, Sergei; Gridnev, Alexei Synthetic Communications, 2011 , vol. 41, # 24 p. 3683 - 3688
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Safety Information
Download SDS|
GHS Pictogram :
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GHS No : GHS05
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Signal Word : Danger
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UN#: 1759
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Class : 8
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Packing Group : Ⅱ
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Hazard Statements : H314
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Precautionary Statements : P260-P264-P280-P301+P330+P331-P304+P340-P363-P405-P501
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Quality Control
Computational Chemistry Data
- TPSA 27.63
- LogP 0.0414
- H_Acceptors 3
- H_Donors 1
- Rotatable_Bonds 0
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